Phosphate process improvements
Advances in technology, equipment and reagents are enhancing phosphate fertilizer production. Optimisation of standard equipment is also vital for ensuring process efficiency.
Advances in technology, equipment and reagents are enhancing phosphate fertilizer production. Optimisation of standard equipment is also vital for ensuring process efficiency.
When candle filter mist eliminators installed in the absorption towers in sulphuric acid plants are not sufficiently wet, problems can occur such as free SO3 at the stack, NOx issues and emission non-compliance. Begg Cousland Envirotec discusses how these problems can be overcome by the installation of an annular wetting ring solution.
The world has seen a number of hydrogen explosions in double absorption plants mostly in the intermediate absorption tower (IAT). To review this increase and to determine the causes, an International Hydrogen Safety Workgroup was formed including major acid plant contractors, major acid producers, and consultants in the sulphuric acid arena. Davis & Associates Consulting explores some of the findings.
Sulphur run-down lines are typically sized by referencing past projects and ‘rules of thumb’. Very little analysis is performed to identify the impacts of slope, fittings, valves, etc. It is critical to maintain an open vapour path from the condenser to the sealing device. CSI has observed problems in the field which appear to be caused by undersized run-down lines and has developed a method of predicting the liquid level in a run-down line that considers the most common elements.
NORAM has recently introduced a patented acid entrainment mitigation device (EMD) to deal with acid mist carryover from sulphuric acid towers.
The purpose of this article is to emphasise the lessons learned by ADNOC Sour Gas in the material upgrading of the Shah sulphur granulation plant due to severe corrosion of the aluminium components. The sulphur granulation plant was commissioned in 2015 and consists of a total of 12 granulating systems used for solidifying and granulating the liquid sulphur. The study focused on the corroded areas, namely the GX plenum chambers, the lower section of the granulator exhaust stack, the scrubber inlet and the discharge ducting.
The precision mixing and granulation of mineral and organic fertilizer ingredients are essential to meet growing market demand for high-value, complex crop fertilizers. Furthermore, the ability to mix and granulate in a single machine offers fertilizer manufacturers both operational and product quality advantages over traditional granulation methods.
Ammonia synthesis catalysts have seen major improvements over the last 100 years, and they are highly optimised with respect to activity, thermal stability, and poisoning resistance. Improving such catalysts even further requires a deep understanding of their structure and the impact of different parameters on performance. Clariant, Johnson Matthey and Topsoe report on their studies and developments in ammonia synthesis catalysts.
Improvements to equipment and materials are driving greater operational performance and higher efficiencies at urea plants. Recent advances are reviewed.
Efficient size preparation and ore transport are key prerequisites for successful potash and phosphate production. We highlight the range of equipment options.