Section: CRUSU Features

This June marks a milestone for this magazine; a platinum jubilee since the very first issue of the magazine was printed in 1953. It began life as the Quarterly Bulletin of the Sulphur Exploration Syndicate. The Syndicate was created in 1952, and was backed by nine major chemical producers, mainly in Britain and the US, who were concerned about dwindling world supplies of sulphur. Though some of these companies have vanished by the wayside over the years, including F.W. Berk and Co. Ltd, British Titan Products, Brotherton & Co., and Charles Tenant & Sons Ltd, others remain household names to this day, including Monsanto, Courtaulds (now part of Akzo-Nobel), and Dunlop (now owned by Goodyear), while Fisons’ fertilizer division was sold to Norsk Hydro in 1982 and today trades as part of Yara.

There is a growing skills gap in the sulphur industry due to the changing nature of the workforce. The traditional ways of doing things are no longer working effectively. Knowledge is lost with retiring subject matter experts (SMEs) and other experienced operations staff leaving a reducing pool of SMEs. In this article a case study reviews how knowledge automation solved the skills gap in a sulphur recovery unit at a major US refinery.

Debopam Chaudhuri of Fluor Daniel India Pvt Ltd and Michiel Baerends of Fluor B.V. Netherlands investigate how SO2 impacts the Claus furnace temperature in an SRU and the ways to mitigate it. This article studies the extent of quenching experienced in the Claus furnace with varying amounts of SO2 in the Claus feed. A case study is presented based on real operating data of a refinery Claus plant with a feed gas cocktail that includes substantial SO2 recovered from a regenerative flue gas desulphurisation unit.

Sulphur dust is one of the greatest hazards when producing and handling solid sulphur, and methods for its suppression are vitally important to prevent fire and explosion.

The centre of gravity of the phosphate industry continues to shift, with Chinese exports less important, and fresh demand coming from India and Brazil.

The 2023 Middle East Sulphur Conference (MEScon 2023) was the biggest sulphur event in the region to date with over 650 attendees representing 23 countries from across the sour gas and sulphur value chain. More than a conference, this annual event offers conversation, collaboration and community, with leaders and experts from across the industry sharing knowledge, best practice and predictions for the future of sulphur.

In 2019 Topsoe launched its ClearView™ technology for WSA and SNOx sulphuric acid plants. ClearView™ is a revolutionary process health monitoring software solution to help sulphuric acid plant operators ensure plants run better, more stable and with less downtime. Now, three years later, ClearView™ has been successfully implemented at two WSA plants and several other chemical plants of Topsoe’s design, with many others in the pipeline. This article focuses on the results and learnings from the first implementation of ClearView™ at a new WSA plant at Anglo American Platinum’s Polokwane smelter in South Africa.

Aged sulphur products can be friable and fragile, which can lead to sulphur dust during handling. Because sulphur dust can lead to dust explosions and excessive wet sulphur contact corrosion, shipping and handling specifications for the safest products are used by producers, shippers and consumers to limit dangerous incidents. Metastable polymeric sulphur in the solid product limits friability and is rarely cited as a measured quantity within sulphur specifications, but often discussed when explaining best handling and forming practices. In this article, ASRL discusses why sulphur tends to be friable and explores several measurements cited in many specification documents, with the purpose of focusing on several modern solid forms. In addition, the measurement of total and extraneous water is explored.

The production of renewable fuels by retrofitting existing refineries and their infrastructure is witnessing exponential growth. The impact on the existing amine, sour water and sulphur recovery units is inevitable. Based on several case studies, Marco van Son, Shashank Gujale and Tammy Chan of Worley Comprimo discuss the various options available to holistically review the sulphur block to determine the impact and mitigation of processing bio-feed.

Sulphur production continues to expand in the Middle East and China both from new refineries and major sour gas projects.