Category: Process

Process and simulation models can be valuable tools when troubleshooting to solve operational issues in sulphur recovery units. Two examples are provided. In the first case study it is shown how a tuned model was useful in troubleshooting an SRU that was experiencing lower than expected recovery efficiency and apparent channelling in the first catalytic converter. In the second case study an SRU simulation tool is used to investigate sulphidic corrosion in a waste heat boiler.

Failure investigations, equipment design and process upgrade projects for SRUs often overlook the impact of water quality. In this article E. Nasat o of Nasato Consulting and L. Huchler of MarTech Systems explore impacts of higher heat transfer rates, control of boiler and condenser water chemistry, conventional equipment design/configurations and monitoring program designs. SRU operators can improve the effectiveness of their failure investigations by implementing a broader, more holistic approach that assesses equipment design, process conditions, operating protocols and water quality issues.

New approaches and novel processing schemes employing oxygen enrichment in sulphur recovery units have been developed and commercialised. In this feature Siirtec Nigi, Linde, Blasch, Fluor and RATE report on their latest developments.

A few years ago DME production from methanol gave a major boost to world methanol demand, with DME being used as a blendstock for LPG. However, demand plateaued and DME has not had the takeoff that its proponents feel it should have. Could new renewable DME processes give it the boost it needs?

thyssenkrupp Industrial Solutions discusses a revamping concept to reduce CO2 emissions by replacing some of the hydrogen in the front end of the ammonia plant with green hydrogen, KBR and Casale report on revamp options to increase the capacity of vintage ammonia plants in the former Soviet Union, Johnson Matthey presents a novel integrated ammonia flowsheet for the production of ammonia, methanol, urea and UFC and Arvos | Schmidtsche Schack discusses the benefits of a new process gas boiler.

G. Bowerbank and W. Blas of Shell Catalysts & Technologies discuss low cost strategies to maximise value at existing gas processing facilities. Changing solvents, introducing advanced column internals or a combination of both are relatively simple and cost-effective options for boosting production or revenue with minimal investment.

An advanced mecaptan removal process has been developed and implemented by RATE. The RATE-Oximer process is an oxidative air-based regeneration process, designed to remove mercaptans from liquid and vapour phases. M. Rameshini of RATE describes the key features of the process and its applications.

N. Temnaya and S. Suvorkin of NIIK report on the modernisation of monopressure (UKL-7) and dual pressure (AK-72) nitric acid plants in Russia and the CIS.

IPCO provides an update on its latest activities, with flexible processes enabling IPCO’s project for the first drum granulation plant in Europe to remain on track despite unprecedented Covid-19 restrictions.

When producing from shale reservoirs, technologies such as horizontal drilling and hydraulic fracturing have been used successfully to access hydrocarbons that otherwise could not be. A less publicised issue in producing from certain hot shale gas reservoirs (T > 100°C) is the presence of H2 S and organo-sulphur compounds in the production fluids. In trying to understand the non-biogenic sources of H2 S, Alberta Sulphur Research Ltd has been involved in studying the decomposition of chemicals used in hydraulic fracturing when exposed to high temperature and high pressure.R.A. Marriott, J.J. Marrugo-Hernandez and R. Prinsloo of ASRL discuss the findings of the study.